Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.1-4
Local Structure and Magnetic Properties of Fe-Mn Nanocrystalline Alloys Fabricated by Mechanical Alloying Technique as a Function of Milling Time
Structural and magnetic properties of Fe50Mn50 nanocrystalline alloys prepared by the mechanical alloying technique (using commercial Fe and Mn powders as the precursors) are studied as a function of milling time, 1 hr to 48 hrs. The nano-crystallite size and shape are examined by using scanning electron microscopy (SEM). The effect of milling time on structural characterization was investigated using X-ray diffractometer (XRD) and extended X-ray absorption fine structure spectroscopy (EXAFS). Both XRD and EXAFS studies showed that the alloying process should be completed after 36 hrs milling. Concerning the magnetic behavior, the data obtained from superconducting quantum interference devices (SQUID) exhibited both magnetic saturation (
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.5-8
Composition Dependence of Perpendicular Magnetic Anisotropy in Ta/CoxFe80-xB20/MgO/Ta (x=0, 10, 60) Multilayers
The perpendicular magnetic anisotropy of sputtered CoFeB thin films covered by MgO was investigated by vibrating sample magnetometry. Three different CoxFe80-xB20 alloys were studied. Under out-of plane magnetic field, the saturation field was found to increase with increasing the Co content. The magnetization and interface anisotropy energy were obtained for all samples. Both showed a marked dependence on the MgO overlayer thickness. In addition, their variations were found to be non-monotonous as a function of the Co concentration.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.9-13
The Effect of Crystal and Non-Crystal Structures on Shielding Material Behaviour Under A.C. Field Excitations
Shielding effects in conductive and magnetic materials were investigated as a function of properties, thickness and diameter. In this work, evaluations on passive conductive and magnetic shield specimens were achieved through experimentation set-up using 50 Hz single and three phase induction field sources. Analysis on material microstructure properties and characteristics of shielding specimens were performed with the use of vibrating sample magnetometer (VSM) and field emission scanning electron microscopy (FESEM). An induction field at 136 μT of single phase system and 50 μT of three phase systems were observed to the shield specimens with the thickness ranged of 0.2 mm to 0.4 mm. It is observed that shield specimen efficiency becomes inversely proportionate to the increment of induction fields. The decrease was attributed to the surface structure texture which relates to the crystallization and non-crystallization geometrical effects.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.14-20
Acceleration of Cell Proliferation and Gene Expression in Human Chondrosarcoma Cells Stimulated by Strong Pulse Magnetic Field
For the treatment of osteoarthritis, pulsed electromagnetic field stimulus has been suggested as a useful therapeutic method in rehabilitative medicine. Most studies have been performed under low-frequency and lowenergy to find out biological properties for stimulating chondrocyte with pulsed magnetic field. In this study, the effect of strong pulse magnetic field on the human chondrosarcoma cells (SW-1353) has been investigated by means of cell counting, morphologies, and gene expression of cartilage extracellular matrix genes. The SW- 1353 cells were exposed under the field intensities of 270, 100, 55, 36, and 26 mTesla during 6 hours a day in 5 consecutive days. The pulse magnetic field with an LRC oscillating signal has the pulse width of 0.126 msec and stimulation period of 1 sec. For the 270 and 100 mTesla stimulation, the cell proliferation significantly increased in 21-24% as compared with the non-stimulated cells. Gene expression of cartilage extracellular matrix genes (
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.21-25
Crystallographic and Magnetic Properties of Nickel Substituted Manganese Ferrites Synthesized by Sol-gel Method
Nickel substituted manganese ferrites, Mn1-xNixFe2O4 (0.0 ≤ x ≤ 0.6), were fabricated by sol-gel method. The effects of sintering and substitution on their crystallographic and magnetic properties were studied. X-ray diffractometry of Mn0.6Ni0.4Fe2O4 ferrite sintered above 523 K indicated a spinel structure; particles increased in size with hotter sintering. The Mössbauer spectrum of this ferrite sintered at 523 K could be fitted as a single quadrupole doublet, indicative of a superparamagnetic phase. Sintering at 573 K led to spectrum fitted as the superposition of two Zeeman sextets and a single quadrupole doublet, indicating both ferrimagnetic and paramagnetic phase. Sintering at 673 K and at 773 K led to spectra fitted as two Zeeman sextets due to a ferrimagnetic phase. The saturation magnetization and the coercivity of Mn0.6Ni0.4Fe2O4 ferrite sintered at 773 K were 53.05 emu/g and 142.08 Oe. In Mn1-xNixFe2O4 (0.0 ≤ x ≤ 0.6) ferrites, sintering of any composition at 773 K led to a single spinel structure. Increased Ni substitution decreased the ferrites' lattice constants and increased their particle sizes. The Mössbauer spectra could be fitted as the superposition of two Zeeman sextets due to the tetrahedral and the octahedral sites of the Fe3+ ions. The variations of saturation magnetization and coercivity with changing Ni content could be explained using the changes of particle size.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.26-29
Crystallographic and Magnetic Properties of MnxFe3-xO4 Powders
MnxFe3-xO4 powders have been fabricated by using sol-gel methods; their crystallographic and magnetic properties were investigated by using X-ray diffraction, scanning electron microscopy, Mössbauer spectroscopy, and vibrating sample magnetometer. The MnxFe3-xO4 ferrite powders annealed at 500 ℃ had a single spinel structure regardless of the Mn2+-doping amount and their lattice constants became larger as the Mn2+ concentration was increased. Their Mössbauer spectra measured at room temperature were fitted with 2 Zeeman sextets due to the tetrahedral and octahedral sites of Fe ions, which made them ferrimagnetic. The magnetic behavior of MnxFe3-xO4 powders showed that the Mn2+-doping amount made their saturation magnetization increase, but there were no severe effects on their coercivities. The saturation magnetization of the MnxFe3-xO4 powder varied from 38 emu/g to 70.0 emu/g and their minimum coercivity was 111.1 Oe.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.30-33
The Magnetic Entropy Change on La0.7Ba0.3Mn1-xFexO3 Compound
The magnetocaloric effect and magnetization behavior have been analyzed in the double-perovskite La0.7Ba0.3Mn1-XFeXO3 compound with the sintering temperature at 1273 K. Samples were fabricated by the conventional solid-state reaction method. X-ray diffraction measurement revealed that all the samples had a single phase in orthorhombic. Detailed investigations of the magnetic entropy behavior of the samples were discussed with the variation of TC. The magnetic entropy changes, ΔSM of approximately 0.36-1.14 J/kg K were obtained in the temperature range of 145-350 K for the La0.7Ba0.3Mn1-XFeXO3 compound. The enhancement of the magnetic entropy change is believed to be due to changes in the microstructure, which changes the magnetic part of the entropy of a solid around the magnetic ordering temperature.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.34-38
The Magnetic and Magnetocaloric Properties of the Perovskite La0.7Ca0.3Mn1-xNixO3
This paper studies the effects of the Mn-site substitution by nickel on the magnetic properties and the magnetocaloric properties of La0.7Ca0.3Mn1-xNixO3 (x = 0, 0.05 and 0.1). The orthorhombic crystal structures of the samples are confirmed by the room temperature X-ray diffraction. The dependence of the Curie temperature (
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.39-42
Structural and Electrical Properties of SrRuO3 thin Film Grown on SrTiO3 (110) Substrate
We studied the structural and electrical properties of SrRuO3 thin films grown on SrTiO3 (110) substrate. High resolution X-ray diffraction measurement of the grown film showed 1) very sharp peaks for SrRuO3 film with a very narrow rocking curve with FWHM = 0.045° and 2) coherent growth behavior having the same in-plane lattice constants of the film as those of the substrate. The resisitivity data showed good metallic behavior; ρ = 63 (205) μΩ·cm at 5 (300) K with a residual resistivity ratio of ~3. The observed kink at ρ(
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.43-49
Pulsed Ferrite Magnetic Field Generator for Through-the-earth Communication Systems for Disaster Situation in Mines
A pulsed ferrite magnetic field generator (FMFG) was designed for the use in the 1000 m long through-theearth (TTE) communication system for mining disaster situations. To miniaturize the TTE system, a ferrite core having 10,000 of permeability was used for the FMFG. Attenuation of the magnetic field intensity from the FMFG (200-turn and 0.18 m diameter) was calculated to be 89.95 dB at 1000 m depth soil having 0.1 S/m of conductivity. This attenuation was lower than 151.13 dB attenuation of 1 kHz electromagnetic wave at the same conditions. Therefore, the magnetic-field was found to be desirable as a signal carrier source for TTE communications as compared to the electromagnetic wave. The designed FMFG generates the magnetic field intensity of 1 × 10−10 Tesla at 1000 m depth. This magnetic field is detectable by compact magnetic sensors such as flux gate or magnetic tunneling junction sensor. Therefore, the miniature FMFG TTE communication system can replace the conventional electromagnetic wave carrier type TTE system and allow reliable signal transmission between rescuer and trapped miners.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.50-56
Comparative Analysis of Flux-Reversal Motors with Six-Switch and Four-Switch Converters
In this paper, the 6-switch inverter for the Flux-Reversal Motor (FRM) has been presented and compared to the 4-switch inverter for the FRM, which is more popular in cost effective applications. To analyze the FRM, we adopted the two-dimensional time-stepped voltage source finite element method (FEM) that uses the actual pulse width modulation (PWM) voltage waveforms as the input data. As the FRM characteristic analysis of actual pwm voltage input, the torque ripples and iron losses (eddy current and hysteresis loss) of the FRM can be precisely calculated. With the simulated and experimental results, the performance and limitations of the 4-switch FRM which is the cost effective drive compared to the 6-switch FRM drive are provided in more detail.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.57-64
Flux Linkage Estimation in a Switched Reluctance Motor Using a Simple Reluctance Circuit
Flux linkage of phase windings is a key parameter in determining the behavior of a switched reluctance motor (SRM)
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.65-73
Optimal Design and Performance Analysis of Permanent Magnet Assisted Synchronous Reluctance Portable Generators
In this paper, design and performance analysis of robust and inexpensive permanent magnet-assisted synchronous reluctance generators (PMa-SynRG) for tactical and commercial generator sets is studied. More specifically, the optimal design approach is investigated for minimizing volume and maximizing performance for the portable generator. In order to find optimized PMa-SynRG, stator winding configurations and rotor structures are analyzed using the lumped parameter model (LPM). After comparisons of stator windings and rotor structure by LPM, the selected stator winding and rotor structure are optimized using a differential evolution strategy (DES). Finally, output performances are verified by finite element analysis (FEA) and experimental tests. This design process is developed for the optimized design of PMa-SynRG to achieve minimum magnet and machine volume as well as maximum efficiency simultaneously.
Journal of Magnetics, 31 Mar 2013, Vol.18 , No.1, pp.74-79
Sampling-Based Sensitivity Approach to Electromagnetic Designs Utilizing Surrogate Models Combined with a Local Window
This paper proposes a sampling-based optimization method for electromagnetic design problems, where design sensitivities are obtained from the elaborate surrogate models based on the universal Kriging method and a local window concept. After inserting additional sequential samples to satisfy the certain convergence criterion, the elaborate surrogate model for each true performance function is generated within a relatively small area, called a hyper-cubic local window, with the center of a nominal design. From Jacobian matrices of the local models, the accurate design sensitivity values at the design point of interest are extracted, and so they make it possible to use deterministic search algorithms for fast search of an optimum in design space. The proposed method is applied to a mathematical problem and a loudspeaker design with constraint functions and is compared with the sensitivity-based optimization adopting the finite difference method.